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Zinc cobalt sulfide (ZnS–CoS) nanoparticles have emerged as promising electrode materials for supercapacitors due to their excellent electrochemical properties. However, achieving both high energy density and power density remains a challenge due to particle agglomeration and instability. In this work, dynamic light scattering-based optimization of ZnS–CoS nanoparticles is carried out by adjusting synthetic parameters including temperature, pH, reagent addition rate, and stabilizer concentration, resulting in significantly smaller particle sizes and improved stability. The optimized ZnS–CoS nanoparticle-based electrode exhibited an exceptional specific capacitance of 1156 F g1, an energy...
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